The aim of this study is to provide to national reference laboratories (NRLs)
the possibility to assess their instrument calibration for the analysis of EU
priority PAHs in standard solutions.
Participation is restricted to officially nominated national reference
laboratories.
Test materials and analytes
Two standard solutions containing the 15+1 EU priority PAHs will be supplied
to the participants for analysis. The individual PAHs are at a concentration
level that allows single dilution (1:10) and addition of internal standards.
The solvent is in both cases acetonitrile. Each ampoule contains approximately
2.5 mL of standard solution.
Please bear in mind that the solutions do not contain any internal standards.
The target analytes are:
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benz[a]anthracene (BaA)
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benzo[a]pyrene (BaP)
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benzo[b]fluoranthene (BbF)
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chrysene (CHR)
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benzo[j]fluoranthene (BjF)
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cyclopenta[cd]pyrene (CPP)
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benzo[k]fluoranthene (BkF)
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dibenz[a,h]anthracene (DhA)
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benzo[c]fluorene (BcL)
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dibenzo[a,e]pyrene (DeP)
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benzo[ghi]perylene (BgP)
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dibenzo[a,h]pyrene (DhP)
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dibenzo[a,i]pyrene (DiP)
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dibenzo[a,l]pyrene (DlP)
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indeno[1,2,3-cd]pyrene (IcP)
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5-methylchrysene (5MC)
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General outline of the exercise
The participants are requested to perform triplicate analyses on the
samples applying a method of their own choice. The preparation of the two
samples (e.g. dilution and addition of internal standards) shall be performed
on two different days.
The national reference laboratories are requested to analyse the samples and
report the results within three weeks after receipt of samples in their
laboratories.
Registration and reporting of results have to be done via the WEB based
interface at
http://www.irmm.jrc.be/imepapp/registerForComparison.action?comparison=77
Deadline for registration is Friday 27 October 2006.